Unfortunately, it was difficult to prepare C PIM 1 membranes with a degree of carbonization below 35% due to the abrupt weight loss of PIM 1 from 0% to 35%. The abrupt weight loss of PIM 1 could be also observed by TGA under N2 flow (Fig. S2, Supplementary Information), although the actual decomposition temperature under N2/H2 flow (95/5 vol%) might be different from the TGA result.

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